N-(tert-Butoxycarbonyl)-1,2-phenylenediamine → HCID 68407867, compound

Participants

Reaction Steps

1-(N-t-butoxycarbonylamino)-2-aminobenzene (Method 17, 1.25 g, 6 mmol) was reacted with 4-bromo-3-fluorobenzoic acid (1.1 g, 5.0 mmol) in an analogous manner to that described in Method 16 to give the title compound, which was used without further purification; Mass Spectrum: (M+H+-Boc) 311.

Provenance & Evidence