HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10612278, compound → HCID 58487999, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10612278 | HCID 10612278 | — |
| Reactant | HCID 58487948 | HCID 58487948 | — |
| Product | HCID 58487999 | HCID 58487999 | 21% |
Reaction Steps
The title compound was prepared following the procedure of Intermediate 17, but starting from 3-(4-bromophenyl)-1-benzofuran (obtained as described in Malamas et al., 2000, J. Med. Chem., 43, 1293-1310). Purification by chromatography (DCM/MeOH 80/20) afforded the title compound as beige solid (21%). HPLC (Condition A), Rt: 3.0 min (HPLC purity: 93.4%). M+(ESI): 293.2
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08247437B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-2976cd667496460fa57d28998b413496 |
| Source note | uspto-grants-2012_08 |