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HRID888195

反应详情

EQUATION

反应方程式

HRID 888195 的结构方程式

REACTANTS

反应物

2
结构：Brc1ccc2c(c1)OCO2
HCID75831

5-Bromobenzo-1,3-dioxole

C7H5BrO2

结构：COc1ccc(N2CCN[C@H](C)C2)cc1OC
HCID58487959

未命名化合物

PRODUCTS

生成物

1
结构：C[C@@H]1CN(c2ccc3c(c2)OCO3)CCN1
HCID11687200

未命名化合物

PROCEDURE

实验过程

The title compound was prepared following the procedure of Intermediate 25, but starting from 4-bromo-1,2-(methylenedioxy)benzene. Purification by flash chromatography (CHCl3/MeOH) gave the title compound as a yellow oil. M+(ESI): 221.2. HPLC (Condition A), Rt: 1.3 min (HPLC purity: 100%).

WORKUP

后处理

  1. customThe title compound was prepared
  2. customPurification by flash chromatography (CHCl3/MeOH)