HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibromomethane → HCID 178426248, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibromomethane | HCID 3024 | — |
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | 1-(4-methylphenyl)imidazole | HCID 5302935 | — |
| Product | HCID 178426248 | HCID 178426248 | — |
Reaction Steps
0.013 mol of 1-(4-methylphenyl)imidazole (2.000 g), 0.0063 mol of dibromomethane (1.099 g; 0.45 ml) and 5 ml of THF are stirred in a pressure tube at room temperature overnight and then at 120° C. for 9 hours. The precipitated solid is filtered off and washed repeatedly with a little tetrahydrofuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08247574B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-b5b18caf86114c2aa35dac328053544f |
| Source note | uspto-grants-2012_08 |