Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ammonia → Didodecylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ammonia | HCID 222 | — |
| 반응물 | 1-Dodecanol | HCID 8193 | — |
| 반응물 | Dodecylamine | HCID 13583 | — |
| 반응물 | Mycophenolic acid glucuronide | HCID 6442661 | — |
| 생성물 | Didodecylamine | HCID 18157 | — |
반응 단계
The same procedure as in Example 15 was repeated except for using 150 g (0.81 mol) of lauryl alcohol in place of stearyl alcohol and using ammonia in an amount of 69 g (4.06 mol), thereby conducting the reaction for 9 h. The initial maximum pressure as measured at a reaction temperature of 220° C. was 21 MPaG. The resultant reaction product was analyzed in the same manner as in Example 15. As a result, it was confirmed that the conversion of the raw alcohol was 96.3%, the selectivity to lauryl amine was 90.9%, the amount of dilauryl amine produced is 8.2%, and the amount of the other by-products produced was 0.6%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08247611B2 |
| 출처 데이터셋 | uspto-grants-2012_08 |
| ORD ID | ord-f4e88b58fd63420a8be510b97d297e8c |
| 출처 메모 | uspto-grants-2012_08 |