反应详情

The same procedure as in Example 15 was repeated except for using 150 g (0.81 mol) of lauryl alcohol in place of stearyl alcohol and using ammonia in an amount of 69 g (4.06 mol), thereby conducting the reaction for 9 h. The initial maximum pressure as measured at a reaction temperature of 220° C. was 21 MPaG. The resultant reaction product was analyzed in the same manner as in Example 15. As a result, it was confirmed that the conversion of the raw alcohol was 96.3%, the selectivity to lauryl amine was 90.9%, the amount of dilauryl amine produced is 8.2%, and the amount of the other by-products produced was 0.6%.

1. customthe reaction for 9 h
2. customas measured at a reaction temperature of 220° C.
3. customThe resultant reaction product