HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → Ethyl 2-(3-hydroxy-4-methoxyphenyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | 3-Hydroxy-4-methoxybenzeneacetic acid | HCID 160562 | — |
| Product | Ethyl 2-(3-hydroxy-4-methoxyphenyl)acetate | HCID 5324706 | — |
Reaction Steps
To 3-hydroxy-4-methoxyphenylacetic acid (5.0 g, 23.8 mmol) in EtOH (100 mL) was added sulfuric acid (1 mL), and the reaction was stirred overnight at room temperature. Once no starting material was seen by analytical tlc, the mixture was concentrated to give the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08247602B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-a612162f54a946f6b691f8cf423f0ff0 |
| Source note | uspto-grants-2012_08 |