2-Bromo-2-methylpropionyl bromide → HCID 67302805, compound

HRID 888839Notes

Reaction equation

HRID 888839 reaction equation
[CH:1]1([NH:8][NH:9][C:10]([O:12][CH2:13][C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)=[O:11])[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[Br:20][C:21]([CH3:26])([CH3:25])[C:22](Br)=[O:23]>>[Br:20][C:21]([CH3:26])([CH3:25])[C:22]([N:8]([CH:1]1[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1)[NH:9][C:10]([O:12][CH2:13][C:14]1[CH:15]=[CH:16][CH:17]=[CH:18][CH:19]=1)=[O:11])=[O:23]

Participants

3

Reactant 2

HCID 886852-Bromo-2-methylpropionyl bromideHCID 67303306HCID 67303306, compound

Product 1

HCID 67302805HCID 67302805, compound

Procedure

Benzyl 2-cycloheptylhydrazinecarboxylate and 2-bromoisobutyryl bromide were used for a similar reaction and treatment as Process 3 of Example 1, and benzyl 2-(2-bromoisobutyryl)-2-cycloheptylhydrazinecarboxylate was obtained as a yellow oil.

Sources & evidence

ORD record
ord-fbdd7ced27da497597905be609625c80
Source dataset
uspto-grants-2012_08
Patent number
US08252781B2

Reaction notes

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