Bromoacetyl bromide → HCID 67303214, compound

HRID 888875Notes

Reaction equation

[CH:1]12[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH:2]1[NH:11][NH:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[N+:19]([O-:21])=[O:20])[CH2:8]2.[Br:22][CH2:23][C:24](Br)=[O:25]>>[Br:22][CH2:23][C:24]([N:11]([CH:2]1[CH:3]2[CH2:9][CH:7]3[CH2:6][CH:5]([CH2:10][CH:1]1[CH2:8]3)[CH2:4]2)[NH:12][C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][C:14]=1[N+:19]([O-:21])=[O:20])=[O:25]

Participants

Reactant 2

HCID 61147Bromoacetyl bromide

HCID 67303093HCID 67303093, compound

Product 1

HCID 67303214HCID 67303214, compound

Procedure

1-(Adamantan-2-yl)-2-(2-nitrophenyl)hydrazine and bromoacetyl bromide were used for a similar reaction and treatment as Process 3 of Example 1, and 1-(2-bromoacetyl)-1-(adamantan-2-yl)-2-(2-nitrophenyl)hydrazine was obtained as a yellow oil.

Sources & evidence

ORD record: ord-2038fec3099b4c769e5bfca129190fc4
Source dataset: uspto-grants-2012_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08252781B2

Reaction notes

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