2-Bromoanisole → HCID 59361515, compound

HRID 888885Notes

Reaction equation

HRID 888885 reaction equation
[CH:1]12[CH2:7][CH:4]([CH2:5][CH2:6]1)[CH2:3][CH:2]2[N:8]1[C:11](=[O:12])[C:10]([CH3:14])([CH3:13])[NH:9]1.Br[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=1[O:22][CH3:23]>>[CH:1]12[CH2:7][CH:4]([CH2:5][CH2:6]1)[CH2:3][CH:2]2[N:8]1[C:11](=[O:12])[C:10]([CH3:14])([CH3:13])[N:9]1[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=1[O:22][CH3:23]

Participants

3

Reactant 2

HCID 113582-BromoanisoleHCID 673032332-(Bicyclo[2.2.1]heptan-2-yl)-4,4-dimethyl-1,2-diazetidin-3-one

Product 1

HCID 59361515HCID 59361515, compound

Procedure

2-(Bicyclo[2.2.1]heptan-2-yl)-4,4-dimethyl-1,2-diazetidin-3-one prepared in Process 5 of Example 78 and 1-bromo-2-methoxybenzene were used for a similar reaction and treatment as Example 181, and the title compound was obtained as a pale yellow oil.

Workup

  1. customwere used for a similar reaction and treatment as Example 181

Sources & evidence

ORD record
ord-3fa3189fbf9745aca2ed80c7068f61f3
Source dataset
uspto-grants-2012_08
Patent number
US08252781B2

Reaction notes

Loading…