3,5-Dimethylpyrazole → HCID 11848918, compound
Reaction equation
Cl[C:2]1[N:11]=[C:10](Cl)[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[N:3]=1.[Cl:13][C:14]1[CH:15]=[C:16]([CH:18]=[CH:19][C:20]=1[Cl:21])[NH2:17].[CH3:22][C:23]1[CH:27]=[C:26]([CH3:28])[NH:25][N:24]=1>>[Cl:13][C:14]1[CH:15]=[C:16]([NH:17][C:10]2[C:9]3[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=3)[N:3]=[C:2]([N:24]3[C:23]([CH3:22])=[CH:27][C:26]([CH3:28])=[N:25]3)[N:11]=2)[CH:18]=[CH:19][C:20]=1[Cl:21]Participants
4
Procedure
Was prepared according to Method B from 2,4-dichloroquinazoline, 3,4-di-chloroaniline and 3,5-dimethylpyrazole. Mp. 223.9-226.5° C.
Workup
- customWas prepared
Sources & evidence
- ORD record
- ord-60549e2019704eff92fdd5284b3eabd0
- Source dataset
- uspto-grants-2012_08
- Patent number
- US08252806B2
Reaction notes
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