3,5-Dimethylpyrazole → HCID 11849087, compound

HRID 889115Notes

Reaction equation

HRID 889115 reaction equation
Cl[C:2]1[N:11]=[C:10](Cl)[C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[N:3]=1.[CH2:13]1[O:22][C:21]2[CH:20]=[CH:19][C:17]([NH2:18])=[CH:16][C:15]=2[O:14]1.[CH3:23][C:24]1[CH:28]=[C:27]([CH3:29])[NH:26][N:25]=1>>[O:22]1[C:21]2[CH:20]=[CH:19][C:17]([NH:18][C:10]3[C:9]4[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=4)[N:3]=[C:2]([N:25]4[C:24]([CH3:23])=[CH:28][C:27]([CH3:29])=[N:26]4)[N:11]=3)=[CH:16][C:15]=2[O:14][CH2:13]1

Participants

4

Reactant 3

HCID 62103,5-DimethylpyrazoleHCID 843101,3-Benzodioxol-5-amineHCID 2528862,4-Dichloroquinazoline

Product 1

HCID 11849087HCID 11849087, compound

Procedure

Was prepared according to Method B from 2,4-dichloroquinazoline, 3,4-(methylenedioxy)aniline and 3,5-dimethylpyrazole. LC-ESI-HRMS of [M+H]+ shows 360.148 Da. Calc. 360.14605 Da, dev. 5.4 ppm.

Workup

  1. customWas prepared

Sources & evidence

ORD record
ord-b1d31d8ae8224f4797ffa6a4ee89aacb
Source dataset
uspto-grants-2012_08
Patent number
US08252806B2

Reaction notes

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