HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → N-(3-Methyl-isoxazol-5-yl)-hydrazinecarboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | Phenyl (3-methylisoxazol-5-yl)carbamate | HCID 22936635 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | N-(3-Methyl-isoxazol-5-yl)-hydrazinecarboxamide | HCID 57927573 | — |
Reaction Steps
Hydrazine hydrate (95 μl) was added to a mixture of (3-methyl-isoxazol-5-yl)-carbamic acid phenyl ester (CA 81479-55-2) (417 mg) and ethanol (5 ml), and the resulting mixture was stirred overnight at room temperature. The precipitate was collected by filtration to obtain the title compound (100 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08252810B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-b9750ba282474cbc9934fa597714b169 |
| Source note | uspto-grants-2012_08 |