HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanamine, 2,2,2-trifluoro- → HCID 178465610, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanamine, 2,2,2-trifluoro- | HCID 9773 | — |
| Reactant | Ethanimidic acid, ethyl ester, hydrochloride (1:1) | HCID 2724290 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178465610 | HCID 178465610 | — |
Reaction Steps
A mixture of 2,2,2-trifluoroethylamine (3 ml), ethyl acetimidate hydrochloride (4.8 g) and ethanol (12 ml) was stirred at room temperature for 90 minutes, and then stirred overnight at 80° C. The reaction mixture was concentrated under reduced pressure to obtain the title compound (6.66 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08252810B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-80ce16101ea54500bf8d07ee72773d25 |
| Source note | uspto-grants-2012_08 |