HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Hydrazinyl-5-(trifluoromethyl)pyridine → 4-Pyridin-3-yl-2-[5-(trifluoromethyl)pyridin-2-yl]-1,2-dihydro-3h-pyrazol-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Hydrazinyl-5-(trifluoromethyl)pyridine | HCID 1477642 | — |
| Reactant | 3-Hydroxy-2-pyridin-3-yl-acrylic acid ethyl ester | HCID 68708088 | — |
| Product | 4-Pyridin-3-yl-2-[5-(trifluoromethyl)pyridin-2-yl]-1,2-dihydro-3h-pyrazol-3-one | HCID 59186928 | — |
Reaction Steps
The compound is prepared analogously to Example 2 from 580 mg (3.00 mmol) of the compound from Example 2A and 558 mg (3.00 mmol) 2-hydrazino-5-(trifluoromethyl)pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08252817B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-43d41458e9f249489f0304243a409c5c |
| Source note | uspto-grants-2012_08 |