HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 59186979, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 68704935 | HCID 68704935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 59186979 | HCID 59186979 | — |
Reaction Steps
200 mg (760 μmol) of the compound from Example 29 are suspended in a mixture of 6 ml ethanol and 4 ml water, 0.6 ml 50% strength sodium hydroxide solution are added and the mixture is heated under reflux for 1 h. After cooling, a weakly acid pH is established with 1 M hydrochloric acid and the precipitate is filtered off with suction, washed with water and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08252817B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-7b09a0412e164788a7731f9a3ffe1759 |
| Source note | uspto-grants-2012_08 |