HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine hydrochloride → HCID 178505480, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine hydrochloride | HCID 11130 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 53390441 | HCID 53390441 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 178505480 | HCID 178505480 | — |
Reaction Steps
In analogy to the procedure described in example 5, 4-{2-[2-(4-chloro-phenyl)-2,4,5,6,7,8-hexahydro-cycloheptapyrazol-3-yl]-2-cyclohexyl-ethoxy}-3-fluoro-benzonitrile (example 14.2) was treated with sodium azide and triethylamine hydrochloride in DMF to give the title compound as white solid. MS: m/e=535.7 [M+H+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08252826B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-cd4351fa07e34cc29cd78423770ec8d8 |
| Source note | uspto-grants-2012_08 |