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HRID889446

反应详情

EQUATION

反应方程式

HRID 889446 的结构方程式

REACTANTS

反应物

2
结构：Cc1cc(Cl)c([N+](=O)[O-])cc1N
HCID292965

4-chloro-2-methyl-5-nitroaniline

C7H7ClN2O2

结构：CCc1ccc([N+](=O)[O-])cc1NS(C)(=O)=O
HCID59313849

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(Cl)c([N+](=O)[O-])cc1NS(C)(=O)=O
HCID67359857

未命名化合物

PROCEDURE

实验过程

Intermediate 79A was prepared from 4-chloro-2-methyl-5-nitroaniline following the procedure employed in the preparation of Intermediate 78A. HPLC: Rt=1.618 min. (CHROMOLITH® column 4.6×50 mm eluting with 10-90% aqueous methanol over 4 min. containing 0.1% TFA, 4 mL/min., monitoring at 220 nm). MS (ES): m/z=265 [M+H]+.

WORKUP

后处理

  1. washHPLC: Rt=1.618 min. (CHROMOLITH® column 4.6×50 mm eluting with 10-90% aqueous methanol over 4 min. containing 0.1% TFA, 4 mL/min., monitoring at 220 nm)