HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-2-methyl-5-nitroaniline → N-(4-chloro-2-methyl-5-nitrophenyl)methanesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-2-methyl-5-nitroaniline | HCID 292965 | — |
| Reactant | N-(2-ethyl-5-nitrophenyl)methanesulfonamide | HCID 59313849 | — |
| Product | N-(4-chloro-2-methyl-5-nitrophenyl)methanesulfonamide | HCID 67359857 | — |
Reaction Steps
Intermediate 79A was prepared from 4-chloro-2-methyl-5-nitroaniline following the procedure employed in the preparation of Intermediate 78A. HPLC: Rt=1.618 min. (CHROMOLITH® column 4.6×50 mm eluting with 10-90% aqueous methanol over 4 min. containing 0.1% TFA, 4 mL/min., monitoring at 220 nm). MS (ES): m/z=265 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08252795B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-ff5e1cd0c2a5486fa1bb29d77912bb22 |
| Source note | uspto-grants-2012_08 |