HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-methoxy-N-(4-methoxybenzyl)ethanamine → HCID 86641385, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-methoxy-N-(4-methoxybenzyl)ethanamine | HCID 3285873 | — |
| Reactant | 6-Chloro-8-(cyclopropyl(4-methoxybenzyl)amino)imidazo[1,2-b]pyridazine-3-carbonitrile | HCID 59313757 | — |
| Product | HCID 86641385 | HCID 86641385 | — |
Reaction Steps
15A was prepared from 2-methoxy-N-(4-methoxybenzyl)ethanamine and 1F following the procedure employed in the preparation of 1G. HPLC: Rt=3.20 min. (CHROMOLITH® column 4.6×50 mm eluting with 10-90% aqueous methanol over 4 min. containing 0.1% TFA, 4 mL/min., monitoring at 220 nm). MS (ES): m/z=372.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08252795B2 |
| Source dataset | uspto-grants-2012_08 |
| ORD ID | ord-7f364d7fe54e45f596a7dc7725d5d54c |
| Source note | uspto-grants-2012_08 |