Formaldehyde → HCID 86641032, compound

Participants

Reaction Steps

Under the same conditions as for the preparation of 2,2-dimethyl-3-(N-morpholino)propanal, 36.8 g (0.44 mol) of 36% aqueous formaldehyde were reacted with 33.4 g (0.46 mol) of isobutyraldehyde and 50.0 g (0.44 mol) of N-cyclohexylmethylamine, and worked up. The product distilled at a top temperature of 69° C. and a pressure of 4·10−2 mbar. Yield: 65.8 g (76% of theory) as a colorless, clear liquid smelling of amine, which had an amine content of 4.94 mmol N/g.

Provenance & Evidence