2-Bromoanisole → HCID 178506687, compound

Participants

Reaction Steps

To a solution of 2-bromoanisole (11.2 g, 60.08 mmol) in heptane (150 mL) was slowly added n-BuLi (1.6 M in hexenes, 36.7 mL). White precipitate formed. The slurry was stirred for 0.5 hrs and was filtered. The solid was washed with pentane and was dried under vacuum. The yield was 6.5 g (94%).

Provenance & Evidence