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HRID889787

反应详情

EQUATION

反应方程式

HRID 889787 的结构方程式

REACTANTS

反应物

3
结构：CC(C)=O
HCID180

Acetone

C3H6O

结构：O=C1C(=O)c2cccc3cccc1c23
HCID6724

Acenaphthenequinone

C12H6O2

结构：Nc1ccc(C(=O)O)cc1N
HCID69263

3,4-Diaminobenzoic acid

C7H8N2O2

PRODUCTS

生成物

1
结构：O=C(O)c1ccc2nc3c(nc2c1)-c1cccc2cccc-3c12
HCID626833

Acenaphtho[1,2-b]quinoxaline-9-carboxylic acid

C19H10N2O2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

500 mL of dimethylformaldehyde was added to a mixture of 10 g of purified acenaphthenequinone and 84 g of 3,4-diaminobenzoic acid. The reactant continued to be stirred at room temperature for 21 hours. The precipitate was filtered to obtain a crude composition. This crude composition was dissolved in heated dimethylformamide, filtered again and purified by washing in dimethylformamide and water.

WORKUP

后处理

  1. filtrationThe precipitate was filtered
  2. customto obtain a crude composition
  3. filtrationfiltered again
  4. custompurified
  5. washby washing in dimethylformamide