HCID 22249928, compound → HCID 22249867, compound

Participants

Reaction Steps

A solution of 4-chloro-3-(2-chloroethyl)-8-mesityl-2-methyl[1,7]naphthyridine (100 mg, 0.28 mmol) in 3-aminopentane (5.0 mL) was stirred at 200° C. for six hours in a sealed tube. After overnight, the residue was purified by silica gel column chromatography (30-50% ethyl acetate/hexane), to give the title compound (104 mg) as pale brown crystals.

Provenance & Evidence