HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69596698, compound → HCID 69596721, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69596698 | HCID 69596698 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 69596721 | HCID 69596721 | — |
Reaction Steps
The title compound, white solid, m.p. 96° C., [α]D20=−97.1° (c=1.0723 in chloroform) and MS: m/e=378.2 (M+H+)] was prepared in accordance with the general method of example 44 from (2S,5R)-3-[5-(4-fluoro-phenyl)-1-(toluene-4-sulfonyl)-pyrrolidin-2-yl]-propionic acid methyl ester [see example 59: colorless oil, [α]D20=−96.4° (c=1.0992 in chloroform) and MS: m/e=406.1 (M+H+)].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06995182B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-843ff4e3af794b8d9fee9fcea6777e34 |
| Source note | uspto-grants-2006_02 |