HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 22559827, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 3-Cyclohexene-1-carboxylic acid | HCID 20903 | — |
| Reactant | P,P-Diphenylphosphinic azide | HCID 199401 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 22559827 | HCID 22559827 | — |
Reaction Steps
A solution of 3-cyclohexenylcarboxylic acid (1 mmol), diphenylphosphoryl azide (1.2 mmol) and triethylamine (2.5 mmol) in toluene was heated at 100° C. for 9 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06995269B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-3aebe6ed39284b3b82d0ab1c136d24fe |
| Source note | uspto-grants-2006_02 |