Triethylamine → HCID 22559827, compound

HRID 890363Notes

Reaction equation

HRID 890363 reaction equation
[CH:1]1([C:7]([OH:9])=O)[CH2:6][CH2:5][CH:4]=[CH:3][CH2:2]1.C1(P([N:24]=[N+]=[N-])(C2C=CC=CC=2)=O)C=CC=CC=1.C(N(CC)CC)C>C1(C)C=CC=CC=1>[N-:24]=[C:7]=[O:9].[CH2:5]1[CH2:4][CH2:3][CH:2]=[CH:1][CH2:6]1

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 209033-Cyclohexene-1-carboxylic acidHCID 199401P,P-Diphenylphosphinic azide

Product 1

HCID 22559827HCID 22559827, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

A solution of 3-cyclohexenylcarboxylic acid (1 mmol), diphenylphosphoryl azide (1.2 mmol) and triethylamine (2.5 mmol) in toluene was heated at 100° C. for 9 hours.

Sources & evidence

ORD record
ord-3aebe6ed39284b3b82d0ab1c136d24fe
Source dataset
uspto-grants-2006_02
Patent number
US06995269B2

Reaction notes

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