HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 890369Generated: October 31, 2026
Hydrochloric Acid → HCID 86759931, compound
https://huagongshe.com/reaction/890369
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | 2-Phenylcyclohexan-1-amine | HCID 544990 | — |
| Product | HCID 86759931 | HCID 86759931 | — |
Reaction Steps
To a solution of 2-phenylcyclohexylamine (2.28 mmol) in methanol was added HCl (4.0 M in dioxane, 0.57 mL). The solution was concentrated and treated with phosgene solution (20% in toluene, 16.0 mL). The reaction was heated at 110° C. overnight and concentrated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06995269B2 |
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| Source dataset | uspto-grants-2006_02 |
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| ORD ID | ord-bfbe4890639d4b41a750273ac3274b6d |
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| Source note | uspto-grants-2006_02 |
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