反应详情

温度

110 °C

To a solution of 2-phenylcyclohexylamine (2.28 mmol) in methanol was added HCl (4.0 M in dioxane, 0.57 mL). The solution was concentrated and treated with phosgene solution (20% in toluene, 16.0 mL). The reaction was heated at 110° C. overnight and concentrated in vacuo.

1. concentrationThe solution was concentrated
2. additiontreated with phosgene solution (20% in toluene, 16.0 mL)
3. concentrationconcentrated in vacuo