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HRID890458

反应详情

EQUATION

反应方程式

HRID 890458 的结构方程式

REACTANTS

反应物

3
结构：CCOC(=O)CBr
HCID7748

Ethyl bromoacetate

C4H7BrO2

结构：O=C([O-])[O-].[Cs+].[Cs+]
HCID10796

Cesium carbonate

CCs2O3

结构：CC(C)(C)[Si](C)(C)Oc1cccc2[nH]ccc12
HCID11593976

4-(t-Butyldimethylsilyloxy)indole

C14H21NOSi

PRODUCTS

生成物

1
结构：CCOC(=O)Cn1ccc2c(O[Si](C)(C)C(C)(C)C)cccc21
HCID68822793

未命名化合物

PROCEDURE

实验过程

In analogy to the procedure described in example 6 a], 4-(tert-butyl-dimethyl-silanyloxy)-1H-indole (EP 206225 A2) was reacted with bromo-acetic acid ethyl ester in the presence of cesium carbonate to obtain the title compound as yellow oil.