HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 21935866, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 86597783 | HCID 86597783 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21935866 | HCID 21935866 | — |
Reaction Steps
In analogy to the procedure described in example 16 c], 6-(4-trifluoromethoxy-phenyl)-4-trifluoromethyl-nicotinic acid methyl ester was treated with lithium aluminium hydride in tetrahydrofuran under reflux conditions for 12 h to give the title compound as yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06995263B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-466bc1b6325f41a48cc4c647572eff73 |
| Source note | uspto-grants-2006_02 |