HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorotrimethylsilane → HCID 9956431, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorotrimethylsilane | HCID 6397 | — |
| Reactant | HCID 9956432 | HCID 9956432 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 9956431 | HCID 9956431 | — |
Reaction Steps
As described for example 1, 171 mg of the polar diastereoisomer of N′-[2-(1H-indol-3-yl)ethyl]-N,N-dimethyl-1-pyridin-2-yl cyclohexane-1,4-diamine were also obtained, dissolved in 2-butanone (20 ml) and converted into the corresponding trihydrochloride with chlorotrimethyl silane (0.297 ml) (171 mg beige solid, mp 225–230° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06998409B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-c3f9190f31af46c9934bcfeca03fffa0 |
| Source note | uspto-grants-2006_02 |