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HRID890693

反应详情

EQUATION

反应方程式

HRID 890693 的结构方程式

REACTANTS

反应物

3
结构：NN.O
HCID24654

Hydrazine hydrate (1:1)

H6N2O

结构：COc1ccc(CC(=N)N)cc1.Cl
HCID12203394

(4-Methoxyphenyl)ethanimidamide--hydrogen chloride (1/1)

C9H13ClN2O

结构：CCOC(=O)C(=O)C(C)NC(C)=O
HCID22245807

Ethyl 3-acetamido-2-oxobutanoate

C8H13NO4

PRODUCTS

生成物

1
结构：COc1ccc(Cc2nnc(C(C)NC(C)=O)c(=O)[nH]2)cc1
HCID135697913

未命名化合物

PROCEDURE

实验过程

Analogously to Example 7A, 5.1 g (25.4 mmol) of 2-(4-methoxyphenyl)ethanamidine hydrochloride (Example 4A) are reacted with 1.53 g (30.5 mmol) of hydrazine hydrate and 7.14 g (38.1 mol) of ethyl 3-(acetylamino)-2-oxobutanoate (Example 6A) to give N-{1-[3-(4-methoxybenzyl)-5-oxo-4,5-dihydro-1,2,4-triazin-6-yl]ethyl}acetamide.