Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 4,5-Diphenyl-4-oxazolin-2-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Carbamic acid, ethyl ester | HCID 5641 | — |
| 반응물 | Benzoin | HCID 8400 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 4,5-Diphenyl-4-oxazolin-2-one | HCID 151245 | — |
반응 단계
Benzoin (31.8 g, 0.15 mol) and urethane (42.79 g, 0.45 mol) were heated to reflux for 3.0 hours. The hot mixture was poured into water (150 mL). Acetone (150 mL) was added and heat was applied until the mixture dissolved. The solution was cooled and filtered, producing a white solid which was used in the next step without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06998415B2 |
| 출처 데이터셋 | uspto-grants-2006_02 |
| ORD ID | ord-47f774078ceb4618a0731b11914bd4c0 |
| 출처 메모 | uspto-grants-2006_02 |