HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22244137, compound → Ethanol, 2-(methyl-4-pyrimidinylamino)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22244137 | HCID 22244137 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | Ethanol, 2-(methyl-4-pyrimidinylamino)- | HCID 23598948 | — |
Reaction Steps
To 9.4 g (50 mmol) 2-[(6-chloropyrimidin-4-yl)-methylamino)ethanol in 50 ml ethanol and 10 ml water, 1 g of a 10% Pd/C paste is added and the resulting mixture is subjected to hydrogenation at a pressure of 60 atmospheres and at room temperature for 8 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07001910B1 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-c0952f1c0c97433f9d0d5d03fe032bfe |
| Source note | uspto-grants-2006_02 |