HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 3013465, compound → HCID 3013467, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 3013465 | HCID 3013465 | — |
| Reactant | HCID 21883390 | HCID 21883390 | — |
| Product | HCID 3013467 | HCID 3013467 | — |
Reaction Steps
The title compound can be prepared from ethyl 9-(4-fluorobenzyl)-9H-β-carboline-3-carboxylate under the similar conditions as those in steps (a) and (b) of example 7. 1H NMR (400 MHz, CD3OD): δ 8.60–8.95 (2H, m), 8.32 (1H, d, J=8 Hz), 7.60–7.75 (2H, m), 6.95–7.45 (5H, m), 5.76 (2H, s), 3.48 (3H, s). HRMS (M+H)+ found: 350.1297. Calcd for C20H17FN3O2: 350.1305.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07001912B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-1645bcb1f6af44909d29e6951376ffa8 |
| Source note | uspto-grants-2006_02 |