HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenyl-2,4-pentanedione → 2-[4-(3,5-Dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenyl-2,4-pentanedione | HCID 233402 | — |
| Reactant | 2-(4-Hydrazinophenyl)ethanol hydrochloride | HCID 22244711 | — |
| Product | 2-[4-(3,5-Dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethanol | HCID 22244655 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 1 of Example 1 from 2-(4-hydrazinophenyl)ethanol hydrochloride and 3-phenylpentane-2,4-dione: MS (ESI) m/z 293 [M+H]+, 1H-NMR (CDCl3) δ 7.45-7.27 (9H, m), 3.79 (2H, t, J=6.6 Hz), 2.87 (2H, t, J=6.6 Hz), 2.32 (3H, s), 2.26 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07001917B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-dab12e71f30049ef90d229c33eed0160 |
| Source note | uspto-grants-2006_02 |