HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Ethylpentane-2,4-dione → 2-[4-(4-Ethyl-3,5-dimethyl-1H-pyrazol-1-yl)phenyl]ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Ethylpentane-2,4-dione | HCID 73761 | — |
| Reactant | 2-(4-Hydrazinophenyl)ethanol hydrochloride | HCID 22244711 | — |
| Product | 2-[4-(4-Ethyl-3,5-dimethyl-1H-pyrazol-1-yl)phenyl]ethanol | HCID 22244619 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 1 of Example 1 from 3-ethyl-2,4-pentanedione and 2-(4-hydrazinophenyl)ethanol hydrochloride: MS (ESI) m/z 245 [M+H]+, 1H-NMR (CDCl3) δ 7.36-7.26 (4H, m), 3.84 (2H, t, J=6.6 Hz), 2.89 (2H, t, J=6.6 Hz), 2.24 (2H, q, J=7.5 Hz), 2.26 (3H, s), 2.22 (3H, s), 1.12 (3H, t, J=7.5 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07001917B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-b047a83665744c8cbae0d318ee2a944d |
| Source note | uspto-grants-2006_02 |