HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 2-[3-(3,5-Dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3-Phenyl-2,4-pentanedione | HCID 233402 | — |
| Reactant | 2-(3-Hydrazinophenyl)ethanol | HCID 22244605 | — |
| Product | 2-[3-(3,5-Dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethanol | HCID 22244546 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 1 of Example 1 from 3-phenyl-2,4-pentanedione and 2-(3-hydrazinophenyl)ethanol (WO 94/07896) hydrochloride: MS (ESI) m/z 293 [M+H]+, 1H-NMR (CDCl3) δ 7.44-7.22 (9H, m), 3.87 (2H, t, J=6.0 Hz), 2.67 (2H, t, J=6.0 Hz), 2.33 (3H, s), 2.15 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07001917B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-22bdb1f5e6ff4af8b6b32b9a98f60d2a |
| Source note | uspto-grants-2006_02 |