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HRID891068

反应详情

EQUATION

反应方程式

HRID 891068 的结构方程式

REACTANTS

反应物

3
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(=O)C(C(C)=O)c1ccccc1
HCID233402

3-Phenyl-2,4-pentanedione

C11H12O2

结构：NNc1cccc(CCO)c1
HCID22244605

未命名化合物

PRODUCTS

生成物

1
结构：Cc1nn(-c2cccc(CCO)c2)c(C)c1-c1ccccc1
HCID22244546

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the procedure described in step 1 of Example 1 from 3-phenyl-2,4-pentanedione and 2-(3-hydrazinophenyl)ethanol (WO 94/07896) hydrochloride: MS (ESI) m/z 293 [M+H]+, 1H-NMR (CDCl3) δ 7.44-7.22 (9H, m), 3.87 (2H, t, J=6.0 Hz), 2.67 (2H, t, J=6.0 Hz), 2.33 (3H, s), 2.15 (3H, s).