HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethoxyphenylboronic acid → HCID 22244610, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethoxyphenylboronic acid | HCID 2734351 | — |
| Reactant | 2-[4-(4-Iodo-3,5-dimethyl-1H-pyrazol-1-yl)phenyl]ethanol | HCID 22244559 | — |
| Product | HCID 22244610 | HCID 22244610 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 1 of Example 12 from 2-[4-(4-iodo-3,5-dimethyl-1H-pyrazol-1-yl)phenyl]ethanol (step 2 of Example 11) and 4-ethoxybenzene boronic acid: MS (ESI) m/z 337 [M+H]+, 1H-NMR (CDCl3) δ 7.43 (2H, d, J=8.6 Hz), 7.33 (2H, d, J=8.6 Hz), 7.24 (2H, d, J=8.7 Hz), 6.98 (2H, d, J=8.7 Hz), 4.08 (2H, q, J=6.9 Hz), 3.91-3.89 (2H, m), 2.93 (2H, t, J=6.6 Hz), 2.31 (3H, s), 2.28 (3H, s), 1.45 (3H, t, J=6.9 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07001917B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-9f3b0ff1822144778af2b381884b4f8a |
| Source note | uspto-grants-2006_02 |