2-Hydroxybenzene-1-sulfonamide → HCID 22244556, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in step 1 of Example 42 from phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate (step 1 of Example 22) and 2-hydroxybenzenesulfonamide [Synth. Commun., 1994, 24, 671]: 1H-NMR (CDCl3) δ 7.74-7.70 (1H, m), 7.48-7.24 (9H, m), 7.15 (2H, d, J=8.2 Hz), 7.02 (1H, d, J=7.7 Hz), 6.93 (1H, t, J=7.6 Hz), 6.16 (1H, br.s), 3.47-3.40 (2H, m), 2.81 (2H, t, J=6.5 Hz), 2.32 (3H, s), 2.23 (3H, s).

Provenance & Evidence