HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-ethoxybenzenesulfonamide → HCID 22244532, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-ethoxybenzenesulfonamide | HCID 3724005 | — |
| Reactant | Phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate | HCID 22244550 | — |
| Product | HCID 22244532 | HCID 22244532 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 1 of Example 42 from phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate (step 1 of Example 22) and 4-ethoxybenzenesulfonamide [Chem. Ber., 1982, 25, 1838]: 1H-NMR (CDCl3) δ 7.74 (2H, d, J=8.9 Hz), 7.47-7.24 (9H, m), 6.95-6.92 (21H, in), 6.40 (1H, br.s), 4.07 (2H, q, J=7.1 Hz), 3.53-3.46 (2H, m), 2.86 (2H, t, J=6.8 Hz), 2.33 (3H, s), 2.26 (3H, s), 1.42 (3H, t, J=7.1 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07001917B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-37f751d3f8bd413188cbacc1386a2df8 |
| Source note | uspto-grants-2006_02 |