3-Sulfamoylbenzamide → 3-({[({2-[4-(3,5-Dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethyl}amino) carbonyl]amino}sulfonyl)benzamide

Participants

Role	Name	HCID	Charge
Reactant	3-Sulfamoylbenzamide	HCID 13668250	—
Reactant	Phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate	HCID 22244550	—
Product	3-({[({2-[4-(3,5-Dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethyl}amino) carbonyl]amino}sulfonyl)benzamide	HCID 22244702	—

Reaction Steps

The title compound was prepared according to the procedure described in step 1 of Example 42 from phenyl 2-[4-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)phenyl]ethylcarbamate (step 1 of Example 22) and 3-(aminosulfonyl)benzamide: 1H-NMR (CDCl3) δ 8.47 (1H, s), 8.01 (2H, d, J=8.9 Hz), 7.60-7.11 (10H, m), 6.70 (1H, br.s), 6.30 (1H, br.s), 3.38-3.35 (2H, m), 2.77-2.71 (2H, m), 2.29 (3H, s), 2.17 (3H, s).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07001917B2
Source dataset	uspto-grants-2006_02
ORD ID	ord-8ddaa57abf7b4c62b1d74e21b6d9491c
Source note	uspto-grants-2006_02