HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Cyanophenylboronic acid → HCID 22244681, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Cyanophenylboronic acid | HCID 2734325 | — |
| Reactant | 2-[4-(4-Iodo-3,5-dimethyl-1H-pyrazol-1-yl)phenyl]ethanol | HCID 22244559 | — |
| Product | HCID 22244681 | HCID 22244681 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 1 of Example 12 from 2-[4-(4-iodo-3,5-dimethyl-1H-pyrazol-1-yl)phenyl]ethanol (step 2 of Example 11) and 3-cyanobenzeneboronic acid: MS (EI) m/z 317 [M]+, 1H-NMR (CDCl3) δ 7.63-7.34 (8H, m), 3.92 (2H, t, J=6.6 Hz), 2.94 (2H, t, J=6.6 Hz), 2.32 (3H, s), 2.29 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07001917B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-db31b655170a4a4eb5ae14ef5e9ed8cf |
| Source note | uspto-grants-2006_02 |