Phenylboronic Acid → HCID 22244653, compound

HRID 891133Notes

Reaction equation

[CH2:1]([C:3]1[C:7](I)=[C:6]([CH3:9])[N:5]([C:10]2[CH:15]=[CH:14][C:13]([CH2:16][CH2:17][OH:18])=[CH:12][CH:11]=2)[N:4]=1)[CH3:2].[C:19]1(B(O)O)[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[CH2:1]([C:3]1[C:7]([C:19]2[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=2)=[C:6]([CH3:9])[N:5]([C:10]2[CH:15]=[CH:14][C:13]([CH2:16][CH2:17][OH:18])=[CH:12][CH:11]=2)[N:4]=1)[CH3:2]

Participants

Reactant 2

HCID 66827Phenylboronic Acid

HCID 22244562HCID 22244562, compound

Product 1

HCID 22244653HCID 22244653, compound

Procedure

The title compound was prepared according to the procedure described in step 1 of Example 12 from 2-[4-(3-ethyl-4-iodo-5-methyl-1H-pyrazol-1-yl)phenyl]ethanol (step 2) and benzeneboronic acid: MS (EI) m/z 306 [M]+.

Sources & evidence

ORD record: ord-4af3572b859a49a991d576b144c697c8
Source dataset: uspto-grants-2006_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07001917B2

Reaction notes

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