HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-BENZENEDISULFONAMIDE → HCID 22244705, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-BENZENEDISULFONAMIDE | HCID 3090044 | — |
| Reactant | Phenyl 2-{4-[5-methyl-4-phenyl-3-(trifluoromethyl)-1H-pyrazol-1-yl]phenyl}ethylcarbamate | HCID 22244671 | — |
| Product | HCID 22244705 | HCID 22244705 | — |
Reaction Steps
The title compound was prepared according to the procedure described in step 1 of Example 42 from phenyl 2-{4-[5-methyl-4-phenyl-3-(trifluoromethyl)-1H-pyrazol-1-yl]phenyl}ethylcarbamate (step 7 of Example 52) and 1,3-benzenedisulfonamide: MS (ESI) m/z 608 [M+H]+, 606 [M−H]−, 1H-NMR (CDCl3) δ 8.62 (1H, br.s), 8.14 (2H, br.s), 7.70 (1H, br.s), 7.39-7.21 (9H, m), 6.18 (1H, br.s), 3.35 (2H, br.s), 2.76 (2H, br.s), 2.15 (3H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07001917B2 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-9d04157716094c248ca7954ddfa18105 |
| Source note | uspto-grants-2006_02 |