4-Chlorobenzenesulfonamide → 4-chloro-N-[({2-[6-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)pyridin-3-yl]ethyl}amino)carbonyl]benzenesulfonamide

Participants

Role	Name	HCID	Charge
Reactant	4-Chlorobenzenesulfonamide	HCID 66824	—
Reactant	phenyl 2-[6-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)pyridin-3-yl]ethylcarbamate	HCID 22244603	—
Product	4-chloro-N-[({2-[6-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)pyridin-3-yl]ethyl}amino)carbonyl]benzenesulfonamide	HCID 22244654	—

Reaction Steps

The title compound was prepared according to the procedure described in step 1 of Example 42 from phenyl 2-[6-(3,5-dimethyl-4-phenyl-1H-pyrazol-1-yl)pyridin-3-yl]ethylcarbamate (step 5) and 4-chlorobenzenesulfonamide: 1H-NMR (CDCl3) δ 8.20 (1H, br.s), 7.83-7.77 (22H, m), 7.63-7.26 (9H, m), 6.68 (1H, br.s), 3.52-3.45 (2H, m), 2.84-2.79 (2H, m), 2.48 (3H, s), 2.67 (3H, s).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07001917B2
Source dataset	uspto-grants-2006_02
ORD ID	ord-6f33020fbdd243239ceb22cd0e14dae9
Source note	uspto-grants-2006_02