Pivaloyl chloride → HCID 22244531, compound

Participants

Reaction Steps

The title compound was prepared according to the procedure described in step 1 of Example 63 from propynylmagnesium bromide, pivaloyl chloride and 2-(4-hydrazinophenyl)ethanol hydrochloride: MS (EI) m/z 334 [M]+, 1H-NMR (CDCl3) δ 7.39-7.29 (4H, m), 6.05 (1H, s), 3.85 (2H, m), 2.90 (2H, m), 2.30 (3H, s), 1.60 (1H, br.s), 1.33 (9H, s).

Provenance & Evidence