HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine → HCID 69663720, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69663720 | HCID 69663720 | — |
Reaction Steps
Acetylation of Oxazolidinone Amine. To the crude oxazolidinone amine residue 16a in DCM at room temperature was added pyridine (30 equivalents) and acetic anhydride (20 equivalents). The solution was stirred for 2 hrs and concentrated in vacua. The oxazolidinone acetamide residue was purified by HPLC to provide pure oxazolidinone acetamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07002020B1 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-9b51ff5f973e4be08c0702b766e1f326 |
| Source note | uspto-grants-2006_02 |